Cambridge ALD: Difference between revisions
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added tool description and alternatives, room numbers |
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|company = Cambridge NanoTech (Veeco) | |company = Cambridge NanoTech (Veeco) | ||
|description = Atomic layer deposition system | |description = Atomic layer deposition system | ||
|location = | |location = Cleanroom 1 (03.2.209A)<br />Cleanroom 2 (03.2.203B) | ||
|primary = Martin | |primary = Martin | ||
|secondary = Karolis | |secondary = Karolis | ||
}} | }} | ||
Two nearly identical Savannah S100-like systems are used for atomic layer deposition of aluminum oxide and hafnium oxide. | |||
Other material deposition alternatives at the [[Main Page|NBI cleanroom]]: | |||
* [[AJA systems]] for sputtering/e-gun evaporation | |||
* [[E-Gun evaporator]] | |||
* [[Edwards evaporator|Edwards thermal evaporator]] | |||
* [[Leica sputter coater]] | |||
* [[MBE|Molecular beam epitaxy system]] | |||
== Growth per cycle (GPC) monitoring == | == Growth per cycle (GPC) monitoring == | ||
<gallery mode="traditional"> | <gallery mode="traditional"> | ||
Image:ALD1.png | Image:ALD1.png|ALD1 HfOx | ||
Image:ALD2.png| | Image:ALD2.png|ALD2 HfOx | ||
</gallery> | </gallery> | ||
Revision as of 11:18, 10 April 2022
 | |
| Essentials | |
|---|---|
| Full name | Savannah S100 (gen. 1) |
| Manufacturer | Cambridge NanoTech (Veeco) |
| Description | Atomic layer deposition system |
| Location | Cleanroom 1 (03.2.209A) Cleanroom 2 (03.2.203B) |
| Responsibility | |
| Primary | Martin |
| Secondary | Karolis |
Two nearly identical Savannah S100-like systems are used for atomic layer deposition of aluminum oxide and hafnium oxide.
Other material deposition alternatives at the NBI cleanroom:
- AJA systems for sputtering/e-gun evaporation
- E-Gun evaporator
- Edwards thermal evaporator
- Leica sputter coater
- Molecular beam epitaxy system
Growth per cycle (GPC) monitoring
-
ALD1 HfOx -
ALD2 HfOx
Available processes
| Deposited material | Precursor | ALD1 | ALD2 | Ref. |
|---|---|---|---|---|
| Hafnium oxide (HfOx, HfO2) | TDMAH tetrakis(dimethylamino)hafnium [(CH3)2N]4Hf  |
Yes | Yes | [1] |
| Aluminum oxide (AlOx, Al2O3) | TMA trimethylaluminum (CH3)3Al  |
Yes | Yes | [2] |
Standard operating procedure
Video on how to operate ALD 1:
Video on how to operate ALD 2:
- Open valve on top of the nitrogen bottle.
- Check nitrogen bottle pressure. Main bottle pressure should be at least 5 bar, line pressure 3 bar (AJA1) 1-2 bar (AJA2).
- If line pressure is outside of range, carefully adjust the regulator valve with the flow set to 20 sccm.
- Make sure the valves of all precursors inside the ALD machine are closed.
- Run recipe Default_cleaning to pump out any residual gas in the gas lines.
- With flow set to 0 the actual flow can be between 0-1 sccm.
- Press the VENT or VENT REACTOR button.
- Open the metal lid.
- Put your sample inside, roughly in the center, away from the gas inlet and outlet.
- Check whether the rubber O-ring is properly seated.
- Close the metal lid. Check that the lid is aligned to sit directly on top of the reactor chamber.
- Press the big round PUMP or PUMP REACTOR button.
- Pressure with flow set to 0: ~5e-2 Torr or lower.
- Place the metal cage on top of the tool.
- Open relevant precursor valves.
- Run your recipe.
- Pressure with 20 sccm N2 flow present: low e-1 Torr.
- ALD1 pulse lengths: H2O ~0.5 s, HfOx TDMAH 0.2 s, AlOx TMA 0.02 s.
- ALD2 pulse lengths: H2O ~0.02 s, HfOx TDMAH 0.2-0.5 s.
- Close precursor valves.
- Press the big round VENT or VENT REACTOR button.
- Place the metal cage on the side of the tool.
- Take out your sample. Check the rubber o-ring.
- Press the big round PUMP or PUMP REACTOR button.
- Close the nitrogen bottle valve on top of the bottle.
- Run recipe Default_heater_set.
Technical notes
- Recipe file location
- ALD1: C:\Savannah\Users\Standard\
- ALD2: C:\Cambridge Nanotech\Recipes\
- Log file location
- ALD1: C:\ALD data. Includes pressure data, screenshot at termination.
- ALD2: C:\Cambridge Nanotech\Log\. Includes pressure and heater temperature data, screenshot at termination, software event logs.
Troubleshooting
- Pressure reading obviously wrong (above 1e3 Torr or below 1e-4 Torr):
- Pressure gauge failure. Unplug the network cable from the small square pressure gauge beneath the chamber and plug it back in. The pressure reading should return to expected values.
- No peak visible during precursor pulse:
- Precursor valves closed. Make sure the relevant precursor valves are open. Consult the labels on the inside of the door.
- Pulse time too short. Select the lowest plotting interval and check whether you can spot a small peak when the automatic valve opens. Increase pulse time as needed.
- Cannot open lid upon venting:
- Chamber pressure still below atmosphere. Confirm pressure reading in software. If pressure is below 5e2 Torr, check whether the nitrogen bottle valve is open.
- Rubber O-ring can get stuck to the lid. Gently but firmly lift the lid. Reseat the O-ring if needed.